Engr. Dulce María Guzmán Bucio

499 Spicer points

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  • Database
    The main doublet was fitted with three symetric Voigt doublets (shown in navy blue, blue and aqua). The spectra was obtained from the surface of a metallic nickel thick sample deposited by thermal sublimation in UHV conditions. Data included in a Master Degree Thesis (Guzmán-Bucio et al. "Oxidation mechanim of metallic nickel," to be published).
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Metallic Ni

    • Elements: Ni

    • Sample composition: Ni

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 15

    • Take-off angle: 90

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    • Software used: Analyzer

    xpsoasis_346_image_100.jpg
  • Database
    The main photoemission line (displayed in blue) was fitted with a Double-Lorentzian lineshape. The spectra was obtained from the surface of a metallic nickel thick sample deposited by thermal sublimation in UHV conditions. Data included in a Master Degree Thesis (Guzmán-Bucio et al. "Oxidation mechanism of metallic nickel," to be published).
    Read more

    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Metallic Ni

    • Elements: Ni

    • Sample composition: Ni

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 15

    • Take-off angle: 90

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    xpsoasis_344_image_100.jpgxpsoasis_344_image_100.jpg
  • Database
    The spectra were obtained from the surface of a metallic nickel thick sample exposed to UHP O2 at 100°C for 8 min in a tubular furnace. The spectra were fitted through the block approach* and are displayed normalized. The main peak (shown in olive green) corresponds to the metallic component; the five doublets are associated to the oxide components. Data included in a Master Degree Thesis (Guzmán-Bucio et al. "Oxidation mechanism of metallic nickel," to be published). * A. Herrera-Gómez, F.S. Aguirre-Tostado, Y. Sun, P. Pianetta, Z. Yu, D. Marshall, R. Droopad, W.E. Spicer, Photoemission from the Sr/Si(001) interface, J. Appl. Phys. 90 (2001) 6070–6072. https://doi.org/10.1063/1.1415758.
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Partially oxidized Ni

    • Elements: Ni, O, C

    • Sample composition: Ni2O3

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 15

    • Take-off angle: various (from top to bottom 90°, 70°, 50°, 40°)

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    xpsoasis_348_image_100.jpg
  • The spectra were obtained from the surface of a metallic nickel thick sample exposed to UHP O2 at 300°C for 20 min in a tubular furnace. The six doublets are associated to NiO.
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: oxidized nickel film

    • Elements: Ni, O, C

    • Sample composition: NiO

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 15

    • Take-off angle: various

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    • Software used: Analyzer

    xpsoasis_501_image_100.png
  • Database
    O 1s spectra was obtained from the surface of a hafnium oxide sample that was deposited by atomic layer deposition over Si(1 0 0) wafers. The component at ~530 eV is associated to Hf-O bonding in hafnium oxide. The component at 532 eV has contributions from the oxygen of the superficial hydroxil groups and from the oxygen in hafnium silicate at the interface HfO2/Si.
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    Information about the sample:

    • Shape: Flat surface

    • Sample material: Hafnium oxide

    • Elements: Hf, O, Si

    • Sample composition: HfO2/HfSiO2/Si

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Take-off angle: 85°

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha 110

    • Spectrometer mode: large angle, small area

    xpsoasis_198_image_100.jpg
  • Fitting of spectra from the core level O 1s from a partially oxidized iron film for different photon energies (6736.5, 6836.5, 6936.5, 7387.5, 7487.5, and 7587.5 eV).
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    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: partially oxidized Fe

    • Elements: Fe,O

    • Sample composition: Fe2O3/Fe

    Data acquisition parameters:

    • Photon source: Synchrotron. Energy

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_956_image_14.jpg
  • The spectra were obtained from a partially oxidized nickel surface and were fitted with the software AAnalyzer(R). The two components at lower binding energy (displayed in olive green) are associated with Ni2O3, the component at higher binding energy (displayed in purple) is associated with adventitious oxygen. Data included in a Master Thesis (Guzmán-Bucio, Dulce M. Mecanismo de oxidación de níquel metálico, Cinvestav, Querétaro).
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    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: Partially oxidized Ni

    • Elements: Ni, O, C

    • Sample composition: Ni2O3

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 15

    • Take-off angle: various

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    • Software used: AAnalyzer

    xpsoasis_350_image_100.jpg
  • Fitting of intrinsic O 1s signals for different photon energies (6736.5, 6836.5, 6936.5, 7387.5, 7487.5, and 7587.5 eV). The original spectra were analyzed under the Active background approach. The intrinsic signals were then obtained by modeling the extrinsic inelastic background accounting for the finite thickness (18 nm) of the oxide layer and X-ray extinction with a modified version of the method proposed by Herrera-Gomez Alberto, The photoemission background signal due to inelastic scattering in conformal thin layers, Queretaro, 2023.
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    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: partially oxidized Fe

    • Elements: Fe,O

    • Sample composition: Fe2O3/Fe

    Data acquisition parameters:

    • Photon source: Synchrotron. Energy

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_953_image_14.jpg
  • The main peak was modeled with two DH lineshapes with their relative areas fixed to the theoretically expected values from the Scofield tables.
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    Files :

    • You must be logged-in to download data

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_968_image_14.jpg
  • Fitting of the Mo 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
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    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_936_image_14.jpg
  • The main peak was modeled with two DH lineshapes with their relative areas fixed to the theoretically expected values from the Scofield tables.
    Read more

    Files :

    • You must be logged-in to download data

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_966_image_14.jpg
  • The spectrum was obtained from a metallic nickel surface. The four doublets are associated to metallic nickel.
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    Information about the sample:

    • Shape: Flat surface

    • Sample material: Metallic Ni

    • Elements: Ni

    • Sample composition: Ni

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 15

    • Take-off angle: 90

    Equipment and analysis software:

    • Brand: ThemoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    • Software used: AAnalyzer

    xpsoasis_387_image_100.jpg
  • Database
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    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: Nickel

    • Elements: Ni

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 15

    • Take-off angle: 90

    Equipment and analysis software:

    • Brand: -

    • Model: -

    • Spectrometer mode: -

    xpsoasis_100_image_100.jpg
  • Fitting of the V 2p photoemission spectrum for a polycrystalline metallic surface, data were published by Lawson et al. (accession #0032402). The apparent asymmetry of the main photoemission line was modeled employing two symmetric Voigt doublets. Another three Voigt doublets were employed to optimize the fitting. The branching ratio of the five components was forced to be equal to the theoretically expected value (0.5165), which was taken from the Scofield tables. Lawson et al., "Study of the First Row Transition Metals by X-ray Photoelectron Spectroscopy", Surface Science Spectra 4, 316-344 (1996) https://doi.org/10.1116/1.1247829Read less
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Polycrystalline metallic Vanadium

    • Elements: V

    • Sample composition: V

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 20

    • Take-off angle: 0

    Equipment and analysis software:

    • Brand: Kratos Analytical, Manchester, UK

    • Model: AXIS HS

    • Spectrometer mode: constant pass energy

    • Software used: Analyzer

    xpsoasis_468_image_100.png
  • Fitting of the V 2p photoemission spectrum for a polycrystalline metallic surface, data were published by Lawson et al. (accession #0032902). The apparent asymmetry of the main photoemission line was modeled employing the Double-Lorentzian asymmetric line-shape. Another three Voigt doublets were employed to optimize the fitting. The branching ratio of the four components was forced to be equal to the theoretically expected value (0.5165), which was taken from the Scofield tables. Lawson et al., "Study of the First Row Transition Metals by X-ray Photoelectron Spectroscopy", Surface Science Spectra 4, 316-344 (1996) https://doi.org/10.1116/1.1247829Read more
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Polycrystalline metallic Vanadium

    • Elements: V

    • Sample composition: V

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 20

    • Take-off angle: 0

    Equipment and analysis software:

    • Brand: Kratos Analytical, Manchester, UK

    • Model: AXIS HS

    • Spectrometer mode: constant pass energy

    • Software used: Analyzer

    xpsoasis_467_image_100.png
  • Fitting of the Rh 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_938_image_14.jpg
  • Fitting of the Pd 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). 
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    xpsoasis_641_image_100.png
  • Fitting of the Ag 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_940_image_14.jpg
  • Database
    Fitting of the Ag 3d photoemission spectrum for the element (research grade). Data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted).Read more
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    Information about the sample:

    • Sample material: Silver

    • Elements: Ag

    • Sample composition: Ag

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 14.34

    • Take-off angle: 90°

    Equipment and analysis software:

    • Software used: AAnalyzer

    xpsoasis_593_image_100.png
  • Fitting of the Sn 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_943_image_14.jpg
  • Database
    Fit if the core level Sn 3d from pure Tin. Data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted).Read more
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: pure Tin

    • Elements: Sn

    • Sample composition: Sn

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    Equipment and analysis software:

    • Software used: AAnalyzer

    xpsoasis_596_image_100.png
  • Fitting of spectra from the core level Fe 2p from a partially oxidized iron film for different photon energies (from top to botton 6836.5, 6736.5, 7587.5, and 7387.5 eV).
    Read more

    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: partially oxidized Fe

    • Elements: Fe,O

    • Sample composition: Fe2O3/Fe

    Data acquisition parameters:

    • Photon source: Synchrotron. Energy

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_955_image_14.jpg
  • Fitting of intrinsic Fe 2p signals for different photon energies (from top to botton 6836.5, 6736.5, 7587.5, and 7387.5 eV). The original spectra were analyzed under the Active background approach. The intrinsic signals were then obtained by modeling the extrinsic inelastic background accounting for the finite thickness (18 nm) of the oxide layer, a semi-infinite metal layer and X-ray extinction with a modified version of the method proposed by Herrera-Gomez Alberto, The photoemission background signal due to inelastic scattering in conformal thin layers, Queretaro, 2023.
    Read more

    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: partially oxidized Fe

    • Elements: Fe,O

    • Sample composition: Fe2O3/Fe

    Data acquisition parameters:

    • Photon source: Synchrotron. Energy

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_954_image_14.jpg
  • The main peak was modeled with two DH lineshapes with their relative areas fixed to the theoretically expected values from the Scofield tables.
    Read more

    Files :

    • You must be logged-in to download data

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_967_image_14.jpg
  • Fitting of the Sb 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_944_image_14.jpg
  • The main peak was modeled with two DH lineshapes with their relative areas fixed to the theoretically expected values from the Scofield tables.
    Read more

    Files :

    • You must be logged-in to download data

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_969_image_14.jpg
  • Fitting of the Zr 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_934_image_14.jpg
  • C 1s spectra was obtained from the surface of a nickel thick sample that was exposed to ultra pure oxygen at 100°C for 8 minutes in the tubular furnace. The peaks at 284.56, 286.50, and 288.15 eV correspond to C-C, C-O, and C=O bonds, all present in adventitious carbon. The peak at 292.62 eV probably is associated to compounds with C-C, C-O and C-H bonds or physisorbed CO2. Finally, the peak at 282.98 eV is diffused carbon, respectively. Data included in a Master Thesis (Guzmán-Bucio, Dulce M. Mecanismo de oxidación de níquel metálico, Cinvestav, Querétaro)
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    Information about the sample:

    • Shape: Flat surface

    • Sample material: Nickel (III) oxide

    • Elements: Ni, O, C

    • Sample composition: Ni2O3.13

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 15

    • Take-off angle: 90°

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha 110

    • Spectrometer mode: small area, large angle

    xpsoasis_203_image_100.jpg
  • The spectrum was obtained from a metallic nickel surface. The four doublets are associated to metallic nickel.
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    Information about the sample:

    • Shape: Flat surface

    • Sample material: Metallic Ni

    • Elements: Ni

    • Sample composition: Ni

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 15

    • Take-off angle: 90

    Equipment and analysis software:

    • Brand: ThemoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    • Software used: AAnalyzer

    xpsoasis_386_image_100.jpg
  • Hf 4f spectrum obtained from a polycrystalline metallic hafnium foil, data were published by Arranz and Palacio (accession #00876-02). The spectrum was fitted with one asymmetric Double-Lorentzian doublet, its branching ratio was forced to be equal to the theoretically expected value taken from the Scofield Tables. A. Arranz and C. Palacio , "Core Level Spectra of Hafnium and Hafnium Nitride (HfN0.9) by XPS", Surface Science Spectra 11, 33-42 (2004) https://doi.org/10.1116/11.20050103Read more
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Metallic Hf

    • Elements: Hf

    • Sample composition: Hf

    Data acquisition parameters:

    • Photon source: Mg Ka

    • Pass energy: 16

    • Take-off angle: 0

    Equipment and analysis software:

    • Brand: SPECS EA

    • Model: 10 model

    • Spectrometer mode: constant pass energy

    • Software used: AAnalyzer

    xpsoasis_459_image_100.png
  • K 2p photoemission spectrum obtained from a KBr surface cleaved in air. The branching ratio of the two doublets were forced to be equal to the theoretically expected values, which were taken from the Scofield tables. The data were published by Vincent Crist. B. Vincent Crist, "KBr Crystal: Cleaved in Air", Surface Science Spectra 1, 292-296 (1992) https://doi.org/10.1116/1.1247654Read more
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Potassium bromide

    • Elements: K, Br

    • Sample composition: KBr

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 25

    • Take-off angle: 0

    Equipment and analysis software:

    • Brand: Surface Science Instruments

    • Model: X-Probe 206

    • Spectrometer mode: constant pass energy

    xpsoasis_461_image_100.png
  • Fitting of the Ge 2p photoemission spectrum for a single crystal surface, data were published by Lawson et al. (accession #0032902). The spectrum was fitted employing one Voigt doublet. The branching ratio was forced to be equal to the theoretically expected value (0.5184), which was taken from the Scofield tables. Lawson et al., "Study of the First Row Transition Metals by X-ray Photoelectron Spectroscopy", Surface Science Spectra 4, 316-344 (1996) https://doi.org/10.1116/1.1247829Read moreRead moreRead more
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Germanium

    • Elements: Ge

    • Sample composition: Ge

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 20

    • Take-off angle: 0

    Equipment and analysis software:

    • Brand: Kratos Analytical, Manchester, UK

    • Model: AXIS HS

    • Spectrometer mode: constant pass energy

    xpsoasis_469_image_100.png
  • Fitting of the Ge 3d photoemission spectrum for a single crystal surface, data were published by Lawson et al. (accession #0032903). The spectrum was fitted employing one Voigt doublet. The branching ratio was forced to be equal to the theoretically expected value (0.6865), which was taken from the Scofield tables. Lawson et al., "Study of the First Row Transition Metals by X-ray Photoelectron Spectroscopy", Surface Science Spectra 4, 316-344 (1996) https://doi.org/10.1116/1.1247829Read less
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    Information about the sample:

    • Shape: Other :single crystal

    • Sample material: Germanium

    • Elements: Ge

    • Sample composition: Ge

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 20

    • Take-off angle: 0

    Equipment and analysis software:

    • Brand: Kratos Analytical, Manchester, UK

    • Model: AXIS HS

    • Spectrometer mode: constant pass energy

    • Software used: Analyzer

    xpsoasis_470_image_100.png
  • Fitting of the Tl 4f photoemission spectrum for a poly crystalline surface, data were published by Engelhard and Baer. (accession #0057302). The spectrum was fitted employing one asymmetric Double-Lorentzian doublet and five Gaussian doublets. The branching ratio was forced to be equal to the theoretically expected value (0.7866), which was taken from the Scofield tables. Data were obtained from: Mark Engelhard and Don Baer , "Third Row Transition Metals by X-ray Photoelectron Spectroscopy", Surface Science Spectra 7, 1-68 (2000) https://doi.org/10.1116/1.1311915
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Metallic Tl

    • Elements: Tl

    • Sample composition: Tl

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 23.5 eV

    • Take-off angle: 45°

    Equipment and analysis software:

    • Brand: Physical Electronics, Incorporated Quantum 2000

    • Model: 11-066

    • Spectrometer mode: constant pass energy

    xpsoasis_488_image_100.png
  • Fitting of the Re 4f photoemission spectrum for a metallic poly crystalline surface, data were published by Engelhard and Baer. (accession #0056902). The spectrum was fitted employing six Voigt doublets. The branching ratio was forced to be equal to the theoretically expected value (0.7871), which was taken from the Scofield tables. Data were obtained from: Mark Engelhard and Don Baer , "Third Row Transition Metals by X-ray Photoelectron Spectroscopy", Surface Science Spectra 7, 1-68 (2000) https://doi.org/10.1116/1.1311915
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Metallic Re

    • Elements: Re

    • Sample composition: Re

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 23.5

    • Take-off angle: 45°

    Equipment and analysis software:

    • Brand: Physical Electronics, Incorporated Quantum 2000

    • Model: 11-066

    • Spectrometer mode: constant pass energy

    • Software used: Analyzer

    xpsoasis_489_image_100.png
  • Fitting of the Bi 4f photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The spectrum was fitted employing one asymmetric Double-Lorentzian doublet and two gaussian doublets. The branching ratio was forced to be equal to the theoretically expected value (0.7863), which was taken from the Scofield tables.
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Metallic Bi

    • Elements: Bi

    • Sample composition: Bi

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 14.25

    • Take-off angle: 90°

    Equipment and analysis software:

    • Software used: AAnalyzer

    xpsoasis_490_image_100.png
  • Fitting of the Lu 4f photoemission spectrum for the element (research grade), data were provided by Vincent Crist (XPS library website, https://xpslibrary.com/). The spectrum was fitted employing five Voigt doublets. The branching ratio was forced to be equal to the theoretically expected value (0.7906), which was taken from the Scofield tables.
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Lu

    • Elements: Lu

    • Sample composition: Lu

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 29.65

    • Take-off angle: 90

    xpsoasis_504_image_100.png
  • Fitting of the Ir 4f photoemission spectrum for the element (research grade), data were provided by Vincent Crist (XPS library website, https://xpslibrary.com/). The spectrum was fitted employing three Voigt doublets. The branching ratio was forced to be equal to the theoretically expected value (0.7866), which was taken from the Scofield tables. The fit needs to be optimized, since it fails to reproduce the data in the circled region (~50 eV).
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    Information about the sample:

    • Shape: Other :element

    • Sample material: Ir

    • Elements: Ir

    • Sample composition: Ir

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 14.25

    • Take-off angle: 90°

    Equipment and analysis software:

    • Software used: Analyzer

    xpsoasis_506_image_100.png
  • Fitting of the Pt 4f photoemission spectrum from a poly crystalline Pt foil, data were published by Engelhard and Baer. (accession #0057102). The spectrum was fitted employing five doublets. The asymmetry of the main line is reproduced with one Double-Lorentzian doublet. The branching ratio was forced to be equal to the theoretically expected value (0.7873), which was taken from the Scofield tables. Data were obtained from: Mark Engelhard and Don Baer, "Third Row Transition Metals by X-ray Photoelectron Spectroscopy", Surface Science Spectra 7, 1-68 (2000) https://doi.org/10.1116/1.1311915Read more
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Pt foil

    • Elements: Pt

    • Sample composition: Pt

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 23.5

    • Take-off angle: 45°

    Equipment and analysis software:

    • Brand: Physical Electronics, Inc.

    • Model: 11-066

    • Spectrometer mode: constant pass energy

    • Software used: AAnalyzer

    xpsoasis_509_image_100.png
  • Fitting of the Pb 4f photoemission spectrum for a poly crystalline surface, data were published by Engelhard and Baer. (accession #0057402). The main photoemission line was fitted using an asymmetric Double-Lorentzian doublet. The branching ratio was forced to be equal to the theoretically expected value (0.7863), which was taken from the Scofield tables. Data were obtained from: Mark Engelhard and Don Baer , "Third Row Transition Metals by X-ray Photoelectron Spectroscopy", Surface Science Spectra 7, 1-68 (2000) https://doi.org/10.1116/1.1311915
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    Information about the sample:

    • Shape: Otherpolycrystal

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Brand: Physical Electronics, Incorporated Quantum 2000

    • Model: 11-066

    • Spectrometer mode: constant pass energy

    • Software used: AAnalyzer

    xpsoasis_580_image_100.jpg
  • Fitting of the Sr 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
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    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_931_image_14.jpg
  • Fitting of the Rb 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
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    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_932_image_14.jpg
  • Fitting of the Y 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
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    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_933_image_14.jpg
  • Fitting of the Nb 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_935_image_14.jpg
  • Fitting of the Ru 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
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    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_937_image_14.jpg
  • metallic palladium sample Fitting of the Pd 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_939_image_14.jpg
  • Fitting of the Cd 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_941_image_14.jpg
  • Fitting of the In 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_942_image_14.jpg
  • Fitting of the Te 3d photoemission spectrum for the element (research grade), data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted). The main peak was fitted with an asymmetric double-Lorentzian lineshape. The total background was modeled with a combination of a Tougaard type background and the interchannel coupling with valence band losses background.
    Read more

    Files :

    • You must be logged-in to download data

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 23.5

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_945_image_14.jpg
  • Fitting of spectra from the core level Fe 2s from a partially oxidized iron film for different photon energies (6736.5, 6836.5, 6936.5, 7387.5, 7487.5, and 7587.5 eV).
    Read more

    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: partially oxidized Fe

    • Elements: Fe,O

    • Sample composition: Fe2O3/Fe

    Data acquisition parameters:

    • Photon source: Synchrotron. Energy

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_957_image_14.jpg
  • Fitting of spectra from the core level Fe 3p and 3s from a partially oxidized iron film for different photon energies (6736.5 and 7487.5 eV).
    Read more

    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: partially oxidized Fe

    • Elements: Fe,O

    • Sample composition: Fe2O3/Fe

    Data acquisition parameters:

    • Photon source: Synchrotron. Energy

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_958_image_14.jpg
  • Fitting of spectra from the core level Fe 3p and 3s from a partially oxidized iron film for different photon energies (6736.5 and 7487.5 eV).
    Read more

    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: partially oxidized Fe

    • Elements: Fe,O

    • Sample composition: Fe2O3/Fe

    Data acquisition parameters:

    • Photon source: Synchrotron. Energy

    Equipment and analysis software:

    • Software used: aanalyzer

    aanalyzer_959_image_14.jpg
  • Database
    The main doublet was fitted with three symetric Voigt doublets (shown in navy blue, blue and aqua). The spectra was obtained from the surface of a metallic nickel thick sample deposited by thermal sublimation in UHV conditions. Data included in a Master Degree Thesis (Guzmán-Bucio et al. "Oxidation mechanim of metallic nickel," to be published).
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Metallic Ni

    • Elements: Ni

    • Sample composition: Ni

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 15

    • Take-off angle: 90

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    • Software used: Analyzer

    xpsoasis_346_image_100.jpg
  • Database
    The main photoemission line (displayed in blue) was fitted with a Double-Lorentzian lineshape. The spectra was obtained from the surface of a metallic nickel thick sample deposited by thermal sublimation in UHV conditions. Data included in a Master Degree Thesis (Guzmán-Bucio et al. "Oxidation mechanism of metallic nickel," to be published).
    Read more

    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Metallic Ni

    • Elements: Ni

    • Sample composition: Ni

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 15

    • Take-off angle: 90

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    xpsoasis_344_image_100.jpgxpsoasis_344_image_100.jpg
  • Database
    The spectra were obtained from the surface of a metallic nickel thick sample exposed to UHP O2 at 100°C for 8 min in a tubular furnace. The spectra were fitted through the block approach* and are displayed normalized. The main peak (shown in olive green) corresponds to the metallic component; the five doublets are associated to the oxide components. Data included in a Master Degree Thesis (Guzmán-Bucio et al. "Oxidation mechanism of metallic nickel," to be published). * A. Herrera-Gómez, F.S. Aguirre-Tostado, Y. Sun, P. Pianetta, Z. Yu, D. Marshall, R. Droopad, W.E. Spicer, Photoemission from the Sr/Si(001) interface, J. Appl. Phys. 90 (2001) 6070–6072. https://doi.org/10.1063/1.1415758.
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: Partially oxidized Ni

    • Elements: Ni, O, C

    • Sample composition: Ni2O3

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 15

    • Take-off angle: various (from top to bottom 90°, 70°, 50°, 40°)

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha110

    • Spectrometer mode: small area, large angle

    xpsoasis_348_image_100.jpg
  • Database
    O 1s spectra was obtained from the surface of a hafnium oxide sample that was deposited by atomic layer deposition over Si(1 0 0) wafers. The component at ~530 eV is associated to Hf-O bonding in hafnium oxide. The component at 532 eV has contributions from the oxygen of the superficial hydroxil groups and from the oxygen in hafnium silicate at the interface HfO2/Si.
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    Information about the sample:

    • Shape: Flat surface

    • Sample material: Hafnium oxide

    • Elements: Hf, O, Si

    • Sample composition: HfO2/HfSiO2/Si

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Take-off angle: 85°

    Equipment and analysis software:

    • Brand: ThermoFisher

    • Model: Alpha 110

    • Spectrometer mode: large angle, small area

    xpsoasis_198_image_100.jpg
  • Database
    Read more

    Files :

    • You must be logged-in to download data

    Information about the sample:

    • Shape: Flat surface

    • Sample material: Nickel

    • Elements: Ni

    Data acquisition parameters:

    • Photon source: Al Ka monochromatic

    • Pass energy: 15

    • Take-off angle: 90

    Equipment and analysis software:

    • Brand: -

    • Model: -

    • Spectrometer mode: -

    xpsoasis_100_image_100.jpg
  • Database
    Fitting of the Ag 3d photoemission spectrum for the element (research grade). Data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted).Read more
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    Information about the sample:

    • Sample material: Silver

    • Elements: Ag

    • Sample composition: Ag

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    • Pass energy: 14.34

    • Take-off angle: 90°

    Equipment and analysis software:

    • Software used: AAnalyzer

    xpsoasis_593_image_100.png
  • Database
    Fit if the core level Sn 3d from pure Tin. Data were provided by Vincent Crist (The use of the spectrum requires acknowledging XPS library website, https://xpslibrary.com/, the data is copyrighted).Read more
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    Information about the sample:

    • Shape: Flat Surface

    • Sample material: pure Tin

    • Elements: Sn

    • Sample composition: Sn

    Data acquisition parameters:

    • Photon source: Al Ka (monochromatic)

    Equipment and analysis software:

    • Software used: AAnalyzer

    xpsoasis_596_image_100.png

Full name:

Dulce María Guzmán Bucio

Title:

Engineer

organization:

Cinvestav

Country:

México

This user is:

Moderator in elements:

Moderator in forums:

Number of post in database:

7

Number of post:

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